NMR Spectra for
Pulse calibration
:
1
H Observe pulse calibration
(0.1% ethylbenzene in CDCl
3
)
High-power
1
H Decoupler Pulse Calibration
(60% C
6
D
6
and 40% p-Dioxane)
Low-power
1
H Decoupler Pulse Calibration
(for CPD) (60% C
6
D
6
and 40% p-Dioxane)
Selective
1
H Observe Pulse calibration
(1,2-dibromopropionic acid in CDCl
3
)
13
C Observe Pulse Calibration
(60% C
6
D
6
and 40% p-Dioxane)
High-power
13
C pulse calibration from decoupler
(100mM
15
N-labeled Urea and
13
C-labeled 100mM CH
3
OH in DMSO-d
6
)
Low-power
13
C pulse calibration from decoupler
(for GARP)(100mM
15
N-labeled Urea and
13
C-labeled 100mM CH
3
OH in DMSO-d
6
)
High-power
15
N pulse calibration from decoupler
(100mM
15
N-labeled Urea and
13
C-labeled 100mM CH
3
OH in DMSO-d
6
)
Low-power
15
N pulse calibration from decoupler
(for GARP) (100mM
15
N-labeled Urea and
13
C-labeled 100mM CH
3
OH in DMSO-d
6
)
31
P Observe Pulse Calibration
(0.0485M triphenylphosphate (TPP) in acetone-d
6
)
