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Sample: EthylBenzene Solvent: CDCl3 Spectrometer: AVANCE 500 Probehead: Inverse Broadband with z-Gradients Experiment: 1H observe pulse calibration Pulse program: zg ( Pulse Diagram) Experiment Time: 4 minute Details: AVANCE Tutorial |
| ACQUISITION | PROCESSING |
| td=32k
o1p=4 sw=10 ns=1 ds=0 d1=10 |
ef using lb=0.3
si=16k |
This pulse calibration is performed using the paropt AU program. pl1 is set to 0dB and p1 is varied from 5 to 24 microseconds using a 1 microsecond step. The first maximum signal stands for the 90 degree pulse (in our case, 10u) that is confirmed by the first null point when the pulse length is doubled (20u).RELATED ITEMS
See list of spectra of EthylBenzeneOBSERVATIONS
PARAMETER SET FILE
Start from the standard PROTON parameter set