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Sample: Triphenylphosphate (TPP) Solvent: Acetone-d6 Spectrometer: AVANCE 500 Probehead: Inverse Broadband with z-Gradients Experiment: 31P observe pulse calibration Pulse program: zg ( Pulse Diagram) Experiment Time: 4 minute Details: AVANCE Tutorial Acquisition: Test Wizard |
| ACQUISITION | PROCESSING |
| td=32k
o1p=-16 sw=50 ns=1 ds=0 d1=10 |
ef using lb=5
si=16k |
This pulse calibration is performed using the paropt AU program. pl1 is set to 0dB and p1 is varied from 8 to 26 microseconds using a 2 microsecond step. The first maximum signal stands for the 90 degree pulse (in our case, about 10-11u) that is confirmed by the first null point when the pulse length is doubled (22u).RELATED ITEMS
See list of spectra of triphenylphosphate (TPP)OBSERVATIONS
PARAMETER SET FILE