Arginine Assignments
NMR experiments for sequence-specific assignment of guanidino side chain spin systems of
arginine
residues in
13
C,
15
N-labeled proteins dissolved in H
2
O.
Experiment
Correlations
2D Arg-H
e
(N
e
)H
g
H
h
2D Arg-H
e
(N
e
)C
z
2D Arg-H
e
N
e
(C
z
)
2D Arg-H
e
(N
e
C
z
)N
h
2D Arg-H
e
(N
e
)C
d
(
96JB59
)
2D Arg-H
e
(N
e
C
d
)C
g
(
96JB59
)
2D Arg-H
e
(N
e
C
d
)H
d
2D Arg-H
h
(N
h
C
z
N
e
)H
e
2D Arg-HC(C)-TOCSY-NEHE
3D HN(CA)HA-gly
(Arg-H
e
N
e(
C
d
)H
d
)