HR-MAS

High resolution magic-angle spinning (HR-MAS) has become an extremely versatile tool to study heterogeneos systems. HR-MAS relies on MAS of the sample to average out to zero magnetic susceptibility differences in the sample and to obtain linewidths approaching those of traditional liquid-state NMR. Thus, HR-MA) provides an easy means of obtaining high resolution spectra for a variety of samples that would otherwise result in poorly resolved spectra. The addition of an HR-MAS probe and a MAS pneumatic unit to a standard high resolution spectrometer is all that is needed to open the gate to the world of hr-MAS spectroscopy and gain access to a vast amount of highly interesting samples.

  • HR-MAS Probes
  • HR-MAS Spectra examples
  • HR-MAS Practical Aspects
  • HR-MAS Applications
  • HR-MAS User Manual 6 Gradient HR-MAS Spectroscopy
    6.1 Magic Angle Gradient Design 6.2 Setting up the magic angle gradient
    7 Application Examples
    7.1 HR-MAS of small organic molecules 7.2 HR-MAS of swollen polymers 7.3 MAS of biological samples 7.4 Gradient HR-MAS spectroscopy 7.5 Water suppression and Diffusion Studies with MAS gradients.