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1D 1H-decoupled 15N spectrum
(using INEPT)

PRELIMINARY SET-UP PARAMETER SET
a conventional 1H-decoupled 15N spectrum with rpar N15INEPT all (the pulse program ineptrd
MODIFY SPECIFIC PARAMETERS

By default, the following parameters are set to: ns=32, ds=2, d1=5, sw=519 and td=32k. Change them if required. The interpulse delay d4 is optimized to 1/(4*1JNH) and d3 as a function of nitrogen multiplicity:


1/(6*1JNH) XH, XH2, XH3 positive
1/(4*1JNH) XH only
1/(3*1JNH) XH, XH3 positive, XH2 negative.
By default, these value are set to 2.8 and 1.9 ms, respectively.
ACQUISITION
PROCESSING
PLOT
OBSERVATIONS

(au_zg)) (proc_1d).

OTHER RELATED VERSIONS
This same experiment can be recorded without refocusing and without decoupling. Only the pulse program might be changed: Non-refocused 1H-coupled using INEPT (ineptnd)
Refocused 1H-coupled using INEPT (ineptpnd)