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Phase-sensitive 2D TOCSY using presaturation
(using MLEV-17)
PRELIMINARY SET-UP
    • PARAMETER SET
    a 2D phase-sensitive 1H-1H TOCSY spectrum using presaturation with (the pulse program mlevphpr
    MODIFY SPECIFIC PARAMETERS
    It is generally recommended that TOCSY experiments be run without sample spinning.

    Finally, set the number of scans as a function of the sample concentration (by default, ns 8 and ds 4).

    ACQUISITION
    PROCESSING
    PLOT
    OBSERVATIONS

    (au_zg)) (proc_2dhom).

    OTHER RELATED VERSIONS A 2D TOCSY pulse program only incorporating a single trim pulse before the MLEV pulse train is also availables :

    Phase-cycle TOCSY experiments
    Gradient-enhanced TOCSY experiments
    Gradient-enhanced TOCSY experiments for H2O