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Phase sensitive 2D TOCSY experiment
(using MLEV-17)
PRELIMINARY SET-UP
    • PARAMETER SET
    a 2D 1H-1H TOCSY spectrum (using MLEV-17) with (the pulse program mlevph
    MODIFY SPECIFIC PARAMETERS
    It is generally recommended that TOCSY experiments be run without sample spinning.

    The power level (pl10) of this mixing time will be set according to the Tutorial: 90º 1H observe pulse calibration.

    Finally, set the number of scans as a function of the sample concentration (by default, ns 8 and ds 4).

    ACQUISITION
    PROCESSING

    Phase correct the spectrum.

    PLOT
    OBSERVATIONS

    (au_getlcosy)) (proc_2dhom).

    OTHER RELATED VERSIONS

    Alternatively, phase-sensitive 2D TOCSY experiments using a z-filtered DIPSI-2 mixing process is also available.

    List of Related Experiments:

    Phase-cycle TOCSY experiments
    Gradient-enhanced TOCSY experiments
    Gradient-enhanced TOCSY experiments for H2O