Go to eNMR
Phase sensitive 2D TOCSY experiment
(using DIPSI-2)

PRELIMINARY SET-UP
  • PARAMETER SET
    a 2D 1H-1H TOCSY spectrum (using DIPSI-2) with and change the pulse program to dipsi2ph
    MODIFY SPECIFIC PARAMETERS
    It is generally recommended that TOCSY experiments be run without sample spinning.

    The power level (pl10) of this mixing time will be set according to the Tutorial: 90º 1H observe pulse calibration.

    Finally, set the number of scans as a function of the sample concentration (by default, ns 8 and ds 4).

    ACQUISITION
    PROCESSING
    Phase correct the spectrum.
    PLOT
    OBSERVATIONS

    (au_getlcosy)) (proc_2dhom).

    OTHER RELATED VERSIONS
    Phase-cycle TOCSY experiments
    Gradient-enhanced TOCSY experiments
    Gradient-enhanced TOCSY experiments for H2O