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PARAMETER SET
a 2D 1H-1H TOCSY spectrum (using DIPSI-2) with and change the pulse program to dipsi2phMODIFY SPECIFIC PARAMETERS
It is generally recommended that TOCSY experiments be run without sample spinning.ACQUISITION
The power level (pl10) of this mixing time will be set according to the Tutorial: 90º 1H observe pulse calibration.
Finally, set the number of scans as a function of the sample concentration (by default, ns 8 and ds 4).
PROCESSING
Phase correct the spectrum.PLOT
OBSERVATIONS
OTHER RELATED VERSIONS(au_getlcosy)) (proc_2dhom).
Phase-cycle TOCSY experiments
Gradient-enhanced TOCSY experiments
Gradient-enhanced TOCSY experiments for H2O