SPECTRA
 

Sample: Sucrose
Solvent: 10% D2O and 90% H2O
Spectrometer: AVANCE 500
Probehead: Inverse Broadband with z-Gradients

Experiment: Water Suppression test
Pulse program: zgpr ( Pulse Diagram)
Experiment Time: 1 minute
Details: AVANCE Tutorial
PARAMETERS
ACQUISITION PROCESSING
td=32k
o1p=4.7 (non spinning)
sw=12
ns=8
ds=2
d1=2
pl9=57
ft
si=16k
COMMENTS
The linewidth is measured at 50% height of the DSS signal and at 10% thereof. The signal to noise is measured on the doublet left to the water signal over a noise range of 1.5 ppm between 5.5ppm and 9.5ppm. Make sure the baseline of this expanded part of the spectra is corrected. On the same doublet the splitting is measured. The splitting must go lower than 40%. This is automatically calculated by typing suppcal. In our case the following values have been obtained: 31.0 Hz at 50%
72.9 Hz at 10%
0% of resolution
154.9 of signal-to-noise.
RELATED ITEMS
See list of spectra of Sucrose
OBSERVATIONS
 
PARAMETER SET FILE