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Sample: Sucrose Solvent: D2O Spectrometer: AVANCE 400 Probehead: Inverse Broadband with z-Gradients Experiment: Phase-sensitive ge-2D HSQC-TOCSY experiment Details: AVANCE Tutorial Pulse program: hsqcgpmlph ( Pulse Diagram) Experiment Time: 30 minutes |
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| ACQUISITION | PROCESSING |
| 2 td=1k
1 td=128w ns=4 d8=120ms |
xfb using MC2=TPPI
2 si=1k 1 si=256w |
OBSERVATIONS
Improved sensitivity is achieved increasing the number of scans. On the other hand, better resolution in the indirect F1 dimension can be achieved by increasing the number of fids to be acquired (1 td) or using linear prediction when processing (MEM=LPfr).PARAMETER SET FILE