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ge-2D 1H-13C HSQC-TOCSY with a z-filter
(phase sensitive)

PRELIMINARY SET-UP
  • PARAMETER SET
    a phase-sensitive ge-2D 1H-13C HSQC-TOCSY spectrum with . Change the pulse program to hsqcgpmlph
    MODIFY SPECIFIC PARAMETERS
    HSQC-TOCSY

    Standard gradient parameters:

  • 80%
  • 30%
  • 20.1%
  • Set the number of scans as a function of the sample concentration (the minimum required is ns 4 and ds 16).

    ACQUISITION
    PROCESSING

    PLOT
    OBSERVATIONS

    (au_getlinv)) (proc_2dinv).

    OTHER RELATED VERSIONS