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Sample: Chentobiose Solvent: CDCl3 Spectrometer: AVANCE 400 Probehead: Inverse Broadband with z-Gradients Experiment: ge-2D multiplicity-edited HSQC experiment Details: AVANCE Tutorial Pulse program: hsqcedgpph ( Pulse Diagram) Experiment Time: 3 minutes |
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| ACQUISITION | PROCESSING |
| 2 td=1k
1 td=64w ns=1 |
xfb using MC2=echo-antiecho
2 si=1k 1 si=256w |
OBSERVATIONS
A only-CH edited HSQC correlation map is obtained setting the d2 value to 1/(4*J)=1.75 msPARAMETER SET FILEImproved sensitivity is achieved increasing the number of scans. On the other hand, better resolution in the indirect F1 dimension can be achieved by increasing the number of fids to be acquired (1 td) or using linear prediction when processing (MEM=LPfr).
Start from the standard HSQCEDGPPH parameter set