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PARAMETER SET
a phase-sensitive ge-2D 1H-13C multiplicity-edited HSQC spectrum with . Change the pulse program to hsqcedgpphMODIFY SPECIFIC PARAMETERS
HSQCACQUISITION PROCESSING
Standard gradient parameters:
Set the evolution period d24 according to multiplicity selection: When optimized to 1/(2*JCH) (ca. 3.5 ms), all XHand XH3 signals are positives whereas XH2 signals are negatives.
Set the number of scans as a function of the sample concentration (the minimum required is ns 1 and ds 16).
PLOT OBSERVATIONS
OTHER RELATED VERSIONS(au_getlinv)) (proc_2dinv).
List of Related Experiments:
Phase-cycle HSQC experiments
Gradient-enhanced HSQC experiments