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ge-2D 1H-13C edited-HSQC with a z-filter
(phase sensitive)

PRELIMINARY SET-UP
  • PARAMETER SET
    a phase-sensitive ge-2D 1H-13C multiplicity-edited HSQC spectrum with . Change the pulse program to hsqcedgpph
    MODIFY SPECIFIC PARAMETERS
    HSQC

    Standard gradient parameters:

  • 30%
  • 80%
  • 20.1%
  • Set the evolution period d24 according to multiplicity selection: When optimized to 1/(2*JCH) (ca. 3.5 ms), all XHand XH3 signals are positives whereas XH2 signals are negatives.

    Set the number of scans as a function of the sample concentration (the minimum required is ns 1 and ds 16).

    ACQUISITION
    PROCESSING

    PLOT
    OBSERVATIONS

    (au_getlinv)) (proc_2dinv).

    OTHER RELATED VERSIONS

    List of Related Experiments:

    Phase-cycle HSQC experiments
    Gradient-enhanced HSQC experiments