Sample: CHCl3 Solvent: Acetone-d6 Spectrometer: AVANCE 500 Probehead: Inverse Broadband with z-Gradients Experiment: 1H lineshape and hump test Pulse program: zg30 ( Pulse Diagram) Experiment Time: 2 minutes Details: AVANCE Tutorial |
ACQUISITION | PROCESSING |
td=32k
o1p=7.7 swh=1000 ns=8 ds=0 d1=2 |
ft using si=16k |
Spinning sidebands are specified with 8 transients and must be below 1% for all standard 5mm and 8mm probes.RELATED ITEMSThe lineshape test is also performed without sample rotation on all probes with watersuppression capability.
See list of spectra of CDCl3OBSERVATIONS
PARAMETER SET FILE
Start from the standard PROHUMP parameter set