Create a new dataset with the edc command.

Read an standard parameter set necessary to record any 3D experiment by typing rpar "filename" all (the active pulse program can be displayed with the edcpul command and the overall pulse sequence can be visualized by typing showpp "pulprog".

See All required offset, pulse and power levels for 3D experiments

Set interpulse delays for each individualized experiment if required. Gradient parameters are already defined and the user must be set the number of scans and dummy scans as a function of sample concentration.

It is advisable to store all acquisition and processing parameters (for instance, with the wpar "filename" all command) to be used later.

Any 3D triple-resonance NMR experiments can be run in automation mode using BioTool.

Any experiment can be run from an already-defined parameter set by typing rpar "filename" all if only a few specific parameters must be changed.