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2D ROESY experiment
(phase sensitive)
PRELIMINARY SET-UP
    • PARAMETER SET
    a 2D 1H-1H ROESY spectrum with (the pulse program roesyph
    MODIFY SPECIFIC PARAMETERS
    It is generally recommended that ROESY experiments be run without sample spinning.

    . Finally, set the number of scans as a function of the sample concentration (by default, ns 16 and ds 4).

    ACQUISITION
    PROCESSING
    . Phase correct the spectrum.
    PLOT
    OBSERVATIONS

    (au_getlcosy)) (proc_2dhom).

    OTHER RELATED VERSIONS

    ROESY pulse programs incorporating a  train of 180(x) 180(-x) pulses as a spin-lock are also availables (see for instance pulprog=roesyph.2). In such cases, p25 is the 180 pulse at pl11 power level and the mixing time is defined equally by p15 (the pulse program automatically calculates the internal l4 loop for spin-lcck). It is advisable that these parameter sets are stored (wpar troesy all) to be used later.

    List of Related Experiments:

    Phase-cycle ROESY experiments
    Gradient-enhanced ROESY experiments
    Gradient-enhanced ROESY experiments for H2O