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magnitude mode ge-2D 1H-15N HMBC
(from the f2 channel)
PRELIMINARY SET-UP
    • PARAMETER SET
    2D 1H-15N HMBC spectrum with . Change the pulse program to hmbcgpndqf

    Change the decoupler nucleus using edasp (set NUC2=15N) and tune and match the probehead.

    MODIFY SPECIFIC PARAMETERS
    HMBC

    Standard gradient parameters:

  • 70%
  • 30%
  • 50.1%

    • Set the number of scans as a function of the sample concentration (the minimum required is ns 2 and ds 16).

    ACQUISITION
    PROCESSING
    PLOT
    OBSERVATIONS

    (au_getlinv)) (proc_2dpl).

    OTHER RELATED VERSIONS

    List of Related Experiments:

    Gradient-enhanced 1H-15N experiments
    Phase-cycled 1H-15N experiments