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2D 1H-13C HMQC-COSY using BIRD with decoupling
(phase sensitive)
PRELIMINARY SET-UP
    • PARAMETER SET
    OPTION A: phase-sensitive 2D HMQC Experiment using BIRD and change the pulse program to hmqcbiphrl

    OPTION B: a phase-sensitive 2D 1H-13C HMQC spectrum using BIRD with . Change the pulse program to hmqcbiphrl

    MODIFY SPECIFIC PARAMETERS
    HMQC-COSY

    Finally, set the number of scans as a function of the sample concentration (by default, ns 8 and ds 16).

    ACQUISITION
    PROCESSING

    PLOT
    OBSERVATIONS

    (au_getlinv)) (proc_2dinv).

    OTHER RELATED VERSIONS
    A 1H-coupled version of the described HMQC-COSY experiment can be recorded only changing the pulse program (pulprog hmqcbindphrl). The pulse program for magnitude-mode 1H-coupled HMQC-COSY experiment is also available (pulprog hmqcbindqfrl).

    List of Related Experiments:

    Phase-cycle inverse experiments
    Gradient-enhanced inverse experiments