a phase-sensitive ge-2D ¹H-¹³C HSQC spectrum with (the pulse program hsqcetgpsi2

HSQC

Standard gradient parameters:

80%

20.1%

11%

-5%

The basic evolution period is optimized to d4=1.72 ms and d24 is optimized according to carbon multiplicity:

1/(4*J_XH) for XH
1/(8*J_XH) for all multiplicities

Set the number of scans as a function of the sample concentration (the minimum required is ns 2 and ds 16).

(au_getlinv)) (proc_2dinv).

List of Related Experiments:

Phase-cycle HSQC experiments
Gradient-enhanced HSQC experiments