Go to eNMR
Selective 1D TOCSY experiment

PRELIMINARY SET-UP
  • Record a conventional 1H spectrum. Note the o1 of the selected resonance.
  • Perform the selective excitation on this selected proton resonance using a selective 270 degree pulse.
  • PARAMETER SET
    a Selective 1D TOCSY spectrum with rpar SELMLZF1H all (the pulse program selmlzf
    MODIFY SPECIFIC PARAMETERS

    A minimum  thirty-two scan cycle is needed (ns=32 and ds=4).

    l4 is the number of delays in the vd-list (z-filter). An example should be:
     
                                0.004s
                                0.016s
                                0.010s
                                0.006s
                                0.004s
                                0.010s
                                0.017s
                                0.011s
                                0.018s
                                0.012s

    ACQUISITION
    PROCESSING
    PLOT
    OBSERVATIONS
    OTHER RELATED VERSIONS