AVANCE Tutorial: 1D CARBON-13 SPECTRUM without NOE

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1D ¹H-decoupled ¹³C spectrum (without NOE)

PRELIMINARY SET-UP

PARAMETER SET

a ¹H-decoupled ¹³C spectrum without NOE with rpar C13IG all (the pulse program zgig30

MODIFY SPECIFIC PARAMETERS

See 90º 13C observe pulse and 90º 1H decouple pulse calibrations.

By default, the following parameters are set to: ns=1024, ds=2, d1=2, sw=331.2 and td=64k. A long recycle period (d1=5*T1(¹³C)) is required when accurate integration is desired.

ACQUISITION

PROCESSING

PLOT

OBSERVATIONS

(au_zg)) (proc_1d).

OTHER RELATED VERSIONS

Also see:

1D 1H-decoupled carbon-13 spectrum
1D 1H-coupled carbon-13 spectrum