AVANCE Tutorial: 1D 1H-Selective-decoupled Carbon-13 Spectrum

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1D ¹H-selective-decoupled ¹³C spectrum

PRELIMINARY SET-UP

PARAMETER SET

a ¹H-decoupled ¹³C spectrum with rpar C13CPD32 all (change the pulse program zgcw30

MODIFY SPECIFIC PARAMETERS

See 90º 13C observe pulse and 90º 1H decouple pulse calibrations.
By default, the following parameters are set to: ns=32, ds=2, d1=2, sw=331.2 and td=64k. Set pl26 to the power required for selective perturbation.

ACQUISITION

PROCESSING

PLOT

OBSERVATIONS

(au_zg)) (proc_1d).

OTHER RELATED VERSIONS

A series of standard parameter sets are available for automation mode: