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ge-2D a,b-HSQC

DESCRIPTION
  • F2-coupled 1H-X correlation and related experiments

  • REQUIREMENTS
    Easy implementation on any AVANCE spectrometer equipped with pulsed field gradients (PFGs) and inverse probehead.
    VERSIONS
    ( 97JB89 , 97JB181 , 98JB445-11 , 98JB435-12 , 98JACS7989 , 98JB325 , 99JMR259-140 )

    Other spin-state selective schemes have been also reported( 00JB221). For instance, a NH2-selected a,b-HSQC experiment to extract 1JNH and 2JHH in NH2 spin systems (02JB27-22 ).

    EXPERIMENTAL DETAILS
    The ge-2D a,b-HSQC experiment is usually recorded in routine and automation modes. Minor changes are required if a predefined parameter set is available.

    More details on practical implementation of ge-2D HSQC experiments on AVANCE spectrometers can be found in the corresponding tutorials:

  • Tutorials: 2D inverse experiments
  • Tutorials: 2D gradient-based inverse experiments
  • SPECTRA
    RELATED TOPICS

    Related experiments:

  • 2D Inverse experiments
  • 2D Inverse gradient-enhanced experiments
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