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REQUIREMENTSF2-coupled 1H-X correlation and related experiments
Easy implementation on any AVANCE spectrometer equipped with pulsed field gradients (PFGs) and inverse probehead.VERSIONS
( 97JB89 , 97JB181 , 98JB445-11 , 98JB435-12 , 98JACS7989 , 98JB325 , 99JMR259-140 )EXPERIMENTAL DETAILSOther spin-state selective schemes have been also reported( 00JB221). For instance, a NH2-selected a,b-HSQC experiment to extract 1JNH and 2JHH in NH2 spin systems (02JB27-22 ).
The ge-2D a,b-HSQC experiment is usually recorded in routine and automation modes. Minor changes are required if a predefined parameter set is available.SPECTRAMore details on practical implementation of ge-2D HSQC experiments on AVANCE spectrometers can be found in the corresponding tutorials:
Tutorials: 2D inverse experiments Tutorials: 2D gradient-based inverse experiments
RELATED TOPICS
Related experiments:
2D Inverse experiments 2D Inverse gradient-enhanced experiments