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The acquisition of the NMR signal is the last step in any NMR experiment. During this period, the NMR signal is recorded in the time domain as a free-induction decay. When acquire 1H signal no other perturbation are usually applied. Thus, 1H signal is recorded with full information about homo- and heteronuclear NMR parameters.REQUIREMENTSOther 1H acquisition schemes are available:
Easy implementation on AVANCE spectrometers.EXPERIMENTAL DETAILS
For more experimental details see Tutorials: Calibration pulses.SYNTAX
The standard way to implement a 1H acquisition period is:RELATED TOPICSin which:
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2 d1
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go=2 ph31
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- go starts data acquisition during an acq period using the acquisition parameters previously defined in eda.
- The number after go (=2) defines the loop to be executed.the number of scans (ns) defines the number of times this loop is repeated.
- ph31 is the receiver phase specified at the end of pulse program and must be cycled in accordance to all pulses involved in the pulse sequence.