a phase-sensitive ge-2D ¹H-¹³C multiplicity-edited HSQC spectrum with (the pulse program hsqcedetgp

HSQC

Standard gradient parameters:

80%

20.1%

Set the evolution period d24 according to multiplicity selection: When optimized to 1/(2*J_CH) (ca. 3.5 ms), all XH and XH3 signals are positives whereas XH2 signals are negatives.

Set the number of scans as a function of the sample concentration (the minimum required is ns 1 and ds 16).

(au_getlinv)) (proc_2dinv).

List of Related Experiments:

Phase-cycle HSQC experiments
Gradient-enhanced HSQC experiments