SPECTRA
 

Sample: Sucrose
Solvent: D2O
Spectrometer: AVANCE 400
Probehead: Inverse Broadband with z-Gradients

Experiment: Conventional 13C spectrum
Details: AVANCE Tutorial
Pulse program: zgpg30 ( Pulse Diagram)
Experiment Time: 5 minutes
PARAMETERS
ACQUISITION PROCESSING
d1=1
td=32k
sw=220
ns=64		 ef using lb=1
si=32k
RELATED ITEMS
 
OBSERVATIONS
Protonated carbon resonances are quickly assigned using a 2D 1H-13C map. On the opther hand, all quaternary carbons can be also assigned from the 2D 1H-13C HMBC spectrum. The multiplicity of all protonated carbons are elucidated from 1D DEPT spectra or froma more suitable 2D multiplicity-edited 1H-13C HSQC experiment.
PARAMETER SET FILE
Start from the standard C13CPD parameter set