Sample: Strychnine Solvent: CDCl3 Spectrometer: AVANCE 400 Probehead: Inverse Broadband with z-Gradients Experiment: Magnitude-mode ge-2D COSY experiment Pulse program: cosygpqf ( Pulse Diagram) Experiment Time: 5 minutes Details: AVANCE Tutorial |
ACQUISITION | PROCESSING |
2 td=1k
1 td=256w ns=1 |
xfb using MC2=QF
sym 2 si=1k 1 si=1k |
The 2D 1H-1H COSY spectrum of strychnine help us in the assignment of the conventional 1H spectrum by defining a series of some spin subsystems.RELATED ITEMS
See list of spectra of strychnineOBSERVATIONS
The concerted use of the 2D 1H-13C HSQC correlation spectra greatly simplifies the assignment procedure.PARAMETER SET FILE
Start from the standard COSYGSSW parameter set