SPECTRA
 

Sample: Cyclosporine
Solvent: C6D6
Spectrometer: AVANCE 500
Probehead: Inverse Broadband with z-Gradients


Experiment: Magnitude-mode ge-2D COSY-DQF experiment
Pulse program: cosygpmfqf ( Pulse Diagram)
Experiment Time: 7 minutes
Details: AVANCE Tutorial
PARAMETERS
ACQUISITION PROCESSING
2 td=1k
1 td=256w
ns=1
xfb using MC2=QF
sym
2 si=1k
1 si=1k
COMMENTS
The 2D 1H-1H COSY spectrum of cyclosporine help us in the assignment of the conventional 1H spectrum by defining a series of some spin subsystems.
RELATED ITEMS
See list of spectra of cyclosporine
OBSERVATIONS
The concerted use of the 2D 1H-13C HSQC correlation spectra greatly simplifies the assignment procedure.
PARAMETER SET FILE
Start from the standard COSYGSSW parameter set