SPECTRA
 

Sample: CHCl3
Solvent: Acetone-d6
Spectrometer: AVANCE 500
Probehead: Inverse Broadband with z-Gradients

Experiment: Inverse test
Pulse program: hmqcndrd1d ( Pulse Diagram)
Experiment Time: 10 minutes
Details: AVANCE Tutorial
Acquisition: Test Wizard
PARAMETERS
ACQUISITION PROCESSING
td=32k
o1p=7.7
o2p=77
swh=1000
ns=8
ds=4
d1=20
d2=2.314m
ft using si=16k
COMMENTS
The central and strong CHCl33 signal is substracted and the carbon satellites are added in this experiment, as we would do a 13C-coupled 1H spectrum. It is very important to use a long d1 (about 20s)and aq (about 16 seconds) periods under non-spinning conditions.
RELATED ITEMS
See list of spectra of CDCl3
OBSERVATIONS
 
PARAMETER SET FILE
Start from the standard HMQC1D parameter set