Sample: CHCl3 Solvent: Acetone-d6 Spectrometer: AVANCE 500 Probehead: Inverse Broadband with z-Gradients Experiment: Inverse test Pulse program: hmqcndrd1d ( Pulse Diagram) Experiment Time: 10 minutes Details: AVANCE Tutorial Acquisition: Test Wizard |
ACQUISITION | PROCESSING |
td=32k
o1p=7.7 o2p=77 swh=1000 ns=8 ds=4 d1=20 d2=2.314m |
ft using si=16k |
The central and strong CHCl33 signal is substracted and the carbon satellites are added in this experiment, as we would do a 13C-coupled 1H spectrum. It is very important to use a long d1 (about 20s)and aq (about 16 seconds) periods under non-spinning conditions.RELATED ITEMS
See list of spectra of CDCl3OBSERVATIONS
PARAMETER SET FILE
Start from the standard HMQC1D parameter set