TUTORIAL: 1D HMQC SPECTRUM

Go to eNMR

1D ¹³C-coupled ¹H-¹³C HMQC spectrum

PRELIMINARY SET-UP

Record a ¹H spectrum.

PARAMETER SET

a conventional 1D ¹H-¹³C HMQC spectra with rpar HMQC1D all (the pulse program hmqcndrd1d

MODIFY SPECIFIC PARAMETERS

By default, the following parameters are set to: d1=20, ns=16, ds=16, sw=12 and td=8k. You can modified them, if required.
d2 is the evolution delay d2 is optimized to 1/(2*¹J_CH) and, by default, set to 2.34 ms (for CHCl₃)

ACQUISITION

PROCESSING

Transform the recorded data with ef (lb=1) and phase the satellites in order to obtain an in-phase doublet.

PLOT

OBSERVATIONS

(au_zg)) (proc_1d).

OTHER RELATED VERSIONS

See list of inverse 1D experiments