HPLC-NMR

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LC-NMR Manual: Examples

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1D ¹H spectrum
• 1D ¹H with presaturation (zgpr)
• 1D ¹H with double presaturation (lc1prf2 | LC1D12)
• 1D ¹H with triple presaturation (lc1prft)
• 1D ¹H with presaturation using shape pulse (zgps)
• 1D ¹H with WET (wet)
• 1D ¹H with WET and CW decoupling on f2 during WET and ACQ (wetdc | LC1DWTDC)
• 1D ¹H with WET and CW decoupling on f2 during WET (wetdw)
• 1D ¹H WET solvent suppression with shape pulse and C-13 decoupling on f2 during WET and AQ for LC isocratic runs (lc2wetdc)
• 1D ¹H WET solvent suppression with shape pulse and C-13 decoupling on f2 during WET and AQ with intermediate preparation scan into second dataset for LC gradient runs with updated shapes (lc2wetdcus | LC2DWTUS)
1D NOESY
• 1D NOESY with presaturation (noesypr1d)
• 1D NOESY with presaturation and CW decoupling on f2 (lc1pncw)
• 1D NOESY with double presaturation and CW decoupling on f2 (lc1pncwfd)
• 1D NOESY with presaturation using shaped pulse and CW decoupling on f2 (lc1pncwps)
• 1D NOESY with double presaturation (lc1pnf2)
• 1D NOESY with multiple presaturation (lc1pnfr)
• 1D NOESY with triple presaturation (lc1pnft)
• 1D NOESY with presaturation using shaped pulse (lc1pnps)
Pseudo-2D-sequence
• Pseudo-2D-sequence for lc-nmr on flow detection (lc2)
• Pseudo-2D-sequence for lc-nmr on flow detection with power-gated decoupling (lc2pg)
• Pseudo-2D-sequence for lc-nmr on flow detection with presaturation (lc2pn)
• Pseudo-2D-sequence for lc-nmr on flow detection with double presaturation (lc2pnf2)
• Pseudo-2D-sequence for lc-nmr on flow detection (lc2pnps)
• Pseudo-2D-sequence for lc-nmr on flow detection with presaturation (lc2pr)
• Pseudo-2D-sequence for lc-nmr on flow detection with double presaturation (lc2prf2)
• Pseudo-2D-sequence for lc-nmr on flow detection with presaturation using shape pulse (lc2ps)
2D homonuclear J-resolved
• 2D J-resolved with double presaturation and cw-decoupling on f2 (lcjrescwfdprqf)
• 2D J-resolved with presaturation and cw-decoupling on f2 (lcjrescwprqf)
• 2D J-resolved with presaturation using shape pulse and cw-decoupling on f2 (lcjrescwpsqf)
• 2D J-resolved with double presaturation (lcjresf2prqf)
• 2D J-resolved with presaturation (lcjresprqf)
• 2D J-resolved with presaturation using shape pulse (lcjrespsqf)
2D TOCSY
• Phase-sensitive 2D TOCSY with double presaturation and cw-decoupling on f2 (lcmlevcwfdpcph)
• Phase-sensitive 2D TOCSY with presaturation and cw-decoupling on f2 (lcmlevcwpcphps)
• Phase-sensitive 2D TOCSY with double presaturation using composite pulse (lcmlevf2pcph)
• Phase-sensitive 2D TOCSY with double presaturation (lcmlevf2phpr | LCML12)
• Phase-sensitive 2D TOCSY with presaturation using shape pulse and composite pulse (lcmlevpcphps)
• Phase-sensitive 2D TOCSY with presaturation using composite pulse (lcmlevpcph)
2D Experiments using WET
• Phase-sensitive 2D COSY using WET (cosydcphwt | COSYDCPHWT)
• Phase-sensitive 2D TOCSY using WET (mlevdcphwt | MLEVDCPHWT)
• Phase-sensitive 2D HSQC using WET (hsqcetgpsiwt | HSQCETGPSIWT)
2D Experiments using single/multiple presaturation using shape pulse
• Phase-sensitive 2D COSY using using single/multiple presaturation (cosycwphps | COSYCWPHPS)
• Magnitude-mode ge-2D COSY using using single/multiple presaturation (cosycwgppsqf)
• Phase-sensitive 2D HSQC using using single/multiple presaturation (hsqcphps)
• Magnitude-mode 2D HMBC using using single/multiple presaturation (hmbcndpsqf)

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