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2D HETCOR experiment with refocusing of chemical shifts
(magnitude mode)
PRELIMINARY SET-UP
    • PARAMETER SET
    a 2D 13C-1H HETCOR spectrum with . Change the pulse program to hxinepqf that
    MODIFY SPECIFIC PARAMETERS
    HETCOR-based

    The evolutions periods must be optimized to d4=1/4J and d3=1/3J, where J is 1JCH (typical value between 140-150 Hz).

    Finally, set the number of scans as a function of the sample concentration (by default, ns 8 and ds 4).

    ACQUISITION
    PROCESSING
    PLOT
    OBSERVATIONS

    (au_getlxhco)) (proc_2dpl).

    OTHER RELATED VERSIONS

    List of Related Experiments:

    Phase-cycle 2D 13C-detected experiments