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PARAMETER SET
a 2D phase-sensitive1H-1H COSY-DQF spectrum with rpar COSYDQFPHSW all (the pulse program cosydfphMODIFY SPECIFIC PARAMETERS
It is generally recommended that COSY-DQF experiments be run without sample spinning.ACQUISITIONSet the number of scans as a function of the sample concentration (by default, ns 16 and ds 4).
PROCESSING
PLOT
OBSERVATIONS
OTHER RELATED VERSIONS(au_getlcosyp)) (proc_2ddqf).
The same scheme can be used to record phase-sensitive 2D COSY experiments
with a multiple-quantum filter. For instance, after reading the standard
parameter set, a
phase-sensitive 2D COSY-TQF (triple-quantum filtered)
experiment
can be run changing the pulse program
(cosyphtf),
the minimum number of scans (ns=24 and ds=24). All other
experimental set-up as described above.
List of Related Experiments:
Phase-cycle COSY experiments
Gradient-enhanced COSY experiments