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2D COSY-DQF experiment
(phase-sensitive)

PRELIMINARY SET-UP
  • PARAMETER SET
    a 2D phase-sensitive1H-1H COSY-DQF spectrum with rpar COSYDQFPHSW all (the pulse program cosydfph
    MODIFY SPECIFIC PARAMETERS
    It is generally recommended that COSY-DQF experiments be run without sample spinning.

    Set the number of scans as a function of the sample concentration (by default, ns 16 and ds 4).

    ACQUISITION
    PROCESSING
    PLOT
    OBSERVATIONS

    (au_getlcosyp)) (proc_2ddqf).

    OTHER RELATED VERSIONS

    The same scheme can be used to record phase-sensitive 2D COSY experiments with a multiple-quantum filter. For instance, after reading the standard parameter set, a phase-sensitive 2D COSY-TQF (triple-quantum filtered) experiment can be run changing the pulse program (cosyphtf), the minimum number of scans (ns=24 and ds=24). All other experimental set-up as described above.
     

    List of Related Experiments:

    Phase-cycle COSY experiments
    Gradient-enhanced COSY experiments