To record a phase-sensitive ge-2D sensitivity-improved HMQC-TOCSY experiment using the echo-antiecho principle, load the parameter set defined for the phase-sensitive ge-2D ¹H-¹³C sensitivity-improved HMQC experiment (by typing rpar inv4etgpsi all, if previously defined) and change the pulse program to hmqcdietgpsi. Modify acquisition parameters if required, and perform data acquisition and data processing as described.

Standard gradient parameters:

80%

40.2%

Modify acquisition parameters if required, and perform data acquisition and data processing as described.