Saccharide NMR
  • Carbohydrates are usually studied using all typical 1D and 2D 1H-1H and 1H-13C NMR experiments used for organic compounds at natural abundance.
  • Spectral simplification by 13C labeling.
    • (HCMe)COH ( 99JB157 )
    • (HCMe)COH-RELAY ( 99JB157 )
    • (H)CMeCOH-HEHAHA ( 99JB157 )
    • H(CMe)COH-HEHAHA ( 99JB157 )
  • 2D COSY-DQF experiment ( 86MRC338 )
  • Miscellaneous experiments:
  • 3D NOESY-TOCSY, selective 2D TOCSY-NOESY and 3D HMQC-NOESY in studies of complex oligosaccharides ( 92JB211 )
  • Band-selective filtered 2D experiments in which the starting point is a DPFGE block to suppress an undesired region ( 00TET393 )
  • Selective 1D HMQC, 1D HSQC-TOCSY, 1D HMQC-NOESY, 1D HSQC-TOCSY-NOESY, and 1D HSQC-TOCSY-NOESY-TOCSY applied to 13C-labeled saccharides ( 00JACS5678 )
  • 3D 13C-edited TOCSY ( 93JMRB204-102 )
  • Solid-State NMR ( 00JACS1102 )