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NMR Experiments for half-integer quadrupolar nuclei

  • MAS
  • Double Rotation (DOR) achives high-resolution spectra of the central transitions by spinning the sample simultaneously at two angles
  • Dynamic-angle spinning (DAS): 2D experiment which achieves isotropic signals in one dimension and quadrupolar-broadened anisotropic powder patterns in the other.
  • MQMAS correlates a multiple-quantum transition with the central transition
  • Satellite transition magic-angle spinning (STMAS) correlates a satellite transition with the central transition
  • Techniques for dipolar-coupled quadrupolar-spin(1/2) pairs

  • TRAPDOR: Transfer of Population in Double Resonance
  • REAPDOR: Rotational-Echo, Adiabatic passage, Double Resonance.
  • Quadrupole Nutation
  • CP-based experiments: HETCOR
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