This angle can also be determined from: DD(NH)-DD(CAHA) cross-correlated rates DD(CAHA)-CSA(CO) cross-correlated rates DD(CAHA)-CSA(N) cross-correlated rates

NMR Experiments (See Tutorials)

• 3D HCACO[N]-E.COSY (hcacogpjc3d | HCACOGPJC3D) - 3J[HAN] via E.COSY
• 3D (H)NNH-TOCSY (hnnhdigp3d | HNNHDIGP3D) - 3J[NN] via quantitative-J
• 3D HNHB - 3J[N-HA] and 3J[N-HB] via quantitative-J