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ge-2D 1H-31P HMBC
(magnitude mode)
PRELIMINARY SET-UP
    • PARAMETER SET
    2D 1H-31PN HMBC spectrum with . Change the pulse program to hmbcgpndqf

    Change the decoupler nucleus using edasp (set NUC2=31P) and tune and match the probehead.

    MODIFY SPECIFIC PARAMETERS
    HMBC

    Standard gradient parameters:

  • 12.34%
  • 12.34%
  • 10%

    • Set the number of scans as a function of the sample concentration (the minimum required is ns 2 and ds 16).

    ACQUISITION
    PROCESSING

    PLOT
    OBSERVATIONS

    (au_getlinv)) (proc_2dpl).

    OTHER RELATED VERSIONS
    2D HMBC experiment can be recorded without gradients (see 2D HMBC experiment).