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Aluminium NMR

PHYSICAL PROPERTIES
 

Isotope
Natural 
Abundance
(%)
Nuclear
Spin
(I)
Magnetogyric
ratio
(107*rad/T*s)
Quadruple 
moment
(1028*Q/m2)
Resonance
frequency
(MHz)
at 11.744T
(500 MHz for 1H)
Relative 
sensitivity
(1H=1.00)
Absolute 
sensitivity
(1H=1.00)
27Al
100
5/2
6.9762715
0.15
130.287
0.21
0.21
 

APPLICATION FIELDS

 27Al NMR spectroscopy is appled on inorganic aluminium-containing compounds (zeolites ...). Solid-state NMR applications are widely used.
NMR REFERENCES
A typical external standard reference is Al(NO3)3 in aqueous solution (absolute frequency of 26.056859 MHz with respect to 100.00 MHz of TMS). Also see IUPAC recommendations for reporting the NMR chemical shits of all nuclei relative to the 1H resonance of TMS (02JMR323-156).
NMR PARAMETERS
NMR EXPERIMENTS
 1D 27Al spectrum
BIBLIOGRAPHY
Interesting reviews: 96ENC742 and B79HAR279, 00ENC691 .
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